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Solubilities Here are some solubility tables for the most common salts used in the production of chlorates and perchlorates. When possible I cited the original sources. Under the tables there are some notes, but for secure safety information, please consult a MSDS (Material Safety Data Sheet) database. Istataneous ice Never get hurted when playing soccer, basket, volley or fishing? :-) Well may be you have used istantaneous ice a strange and wonderful bag that gets cold if you break the inner bubble. This is how it works! Lead Dioxide Anode The lead dioxide anode is an electrode of massive lead dioxide in an extremely hard and dense form. It is produced by electrodeposition on a suitable base material from an aqueous lead salt bath. This form of lead dioxide is of increasing interest as an inert anode in electrochemical processes. Its many favorable properties make it a promising substitute for the platinum anode. Ceramic Substrate Lead Dioxide Anode In this page I describe how to make a ceramic substrate lead dioxide anode following the ideas of some patents regarding inert substrate electrodes, but without the problematic, labour intensive procedure of making it conductive.
A brief history: to produce chlorates and/or perchlorates by electrolysis, one needs an inert anode, which has to resist the chlorine action. Many solutions are available. Platinum is the king of materials, but it is not cheap. Graphite is good for chlorates and one can use carbon rods instead, available as gouging rods. They are cheap, not always simple to find and unuseable for perchlorate production. Plastic Substrate Lead Dioxide Anode This (probably) is the first web-published attempt to make a lead dioxide (PbO2) anode using a plastic substrate. I published a set of pictures on year 2000 without comments, so some of you may already saw them. There are other my plastic anode pictures in Micheal Mc Ardle site of the very first attempt I made (1999?). |
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